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Table of contents

This work investigates cultivating the red-pigmented yeast Phaffia rhodozyma in sweet sorghum juice SSJ to assess the production of astaxanthin as a potential biorefinery co-product. Shake flask cultures on defined sugar medium indicated that all three sugars sucrose, glucose, and fructose could be consumed with adequate nitrogen and nutrient supplementation.

Only modest biomass growth and astaxanthin production could be achieved in SSJ without nitrogen supplementation; however, combining nitrogen supplementation with yeast extract in diluted SSJ could metabolize all sugars present in h. A 2 L bioreactor trial with full strength i. Further process optimization is needed since glucose metabolism was incomplete in undiluted SSJ. Electrolysis of toilet wastewater with TiO2-coated semiconductor anodes and stainless steel cathodes is a potentially viable onsite sanitation solution in parts of the world without infrastructure for centralized wastewater treatment.

In addition to treating toilet wastewater, pilot-scale and bench-scale experiments demonstrated that electrolysis can remove phosphate by cathodic precipitation as hydroxyapatite at no additional energy cost. While calcium was critical for phosphate removal, magnesium and bicarbonate had only minor impacts on phosphate removal rates at concentrations typical of toilet wastewater. Pilot-scale systems are currently operated under similar conditions, suggesting that phosphate removal can be viewed as an ancillary benefit of electrochemical wastewater treatment, adding utility to the process without requiring additional energy inputs.

Further value may be provided by designing reactors to recover precipitated hydroxyapatite for use as a low solubility phosphorus-rich fertilizer. Larger interlayer distance and higher doping efficiency of heteroatoms are considered to be the two most effective solutions to modulate the electronic structure of carbon materials to achieve improved electrochemical storage performances. Here, an innovative popping process is applied to puff biomaterials, i. Thus, well-defined and interconnected three-dimensional pores are constructed within the biomaterial-derived carbon aerogels after a one-step pyrolysis process.

These N, S dual-doped carbon nanosheets, derived from both rice and wheat, display outstanding energy storage performances, thus demonstrating the general ability or possibility of the traditional Chinese popping strategy to convert other biomaterials into similar carbon nanosheets with expanded interlayer distance and enhanced heteroatom doping efficiency. The economically viable synthesis of levulinic acid LA , a promising and valuable renewable biomass-derived platform for bioproducts, with high carbon efficiency is a challenge.

A direct and highly effective catalytic system for conversion of xylose residues XRs into LA under mild conditions by using FeCl3 as catalyst and cheaply available NaCl as promoter has been developed. The NaCl solution exhibits high carbon efficiency in LA The experimental results demonstrated that the presence of NaCl caused no distinctive changes on reaction pathways but increased the dissolution rate and the hydrolysis rate of XRs cellulose.

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Moreover, further integration of our degradation process with a reactive extraction step makes energy-efficient separation of LA. The NaCl solutions easily and efficiently extracted LA into LA-derived solvent 2-methyltetrahydrofuran from aqueous solutions. The efficiency and integration of the reaction process presented a great potential for LA production from renewable biomass with the aid of concentrated seawater. A series of nanocrystalline titanium Ti sub-oxides, including TiO, Ti2O3, Ti3O5, and Ti4O7, with high surface area and activity are successively synthesized using a facile synthesis method that combines the sol—gel and the energy-efficient vacuum-carbothermic SG-VC processes.

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The phase compositions of the resulting powders are primarily determined by two process parameters, including the carbothermic carbon C content, expressed as the C-to-Ti molar ratio of the reactant powder, and the cooling protocol. Examples of the resulting MP Ti4O7 powder exhibiting outstanding pseudocapacitive and oxygen evolution reaction catalytic behaviors are demonstrated.

Nanomaterials that show aggregation-induced emission AIE have tremendous potential in sensors, bioimaging, phototherapy and organic light-emitting diodes. Although big progress have been achieved in developing AIE nanomaterials and their applications, one downside of most previously described AIE nanomaterials is that they required the complicated organic synthesis of precursor molecules and several preparative steps. CEL-NPs showed nice colloidal stability in acidic environment and at low temperature.

This work opens up new possibilities for preparation of AIE nanomaterials and also provides a new high value-added routing for utilization of CEL. A cation-exchange metal—organic framework sorbent with high adsorption capacity, active anionic surface, available adsorptive sites, good response in magnetic field and also available enclosed space between the particles for encapsulation of the analyte was in situ prepared by magnetization of a metal organic framework structure of aluminum named as MIL Al.

The units of magnetic MIL Al was synthesized by embedding method under hydrothermal condition and well characterized. The face-centered central composite design was applied for optimizing the adsorption conditions, and the effective parameters were obtained as pH of 6. The catalytic performance of graphitic carbon nitride g-C3N4 is significantly affected by its microstructure and intrinsic defects.

Here, rodlike g-C3N4 RCN with hierarchical structure and fewer defects is fabricated through an ultrasound-assisted molecular rearrangement strategy. Rodlike supramolecular precursors are formed by rearrangement of melem through ultrasound in water.

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No expensive or hazardous reagent is involved in this process. The decrease in defects has been confirmed by powder X-ray diffraction, Fourier transform infrared, and X-ray photoelectron spectroscopy. The special hierarchical structure provides RCN with significantly increased surface area and enhanced efficiency of light harvesting. The decrease in defects broadens the visible-light responsive range, suppresses the recombination of electron—hole pairs, and enhances the electric conductivity.

Pseudocapacitive electrode materials that involve a Faradaic process are being used in capacitive deionization CDI. The benefits of coupling MnO2 with the CNT—CS matrix are attributed to the mesoporosity to facilitate ion transport, hydrophilicity to increase the electrochemical contact, and good electrical conductivity to improve the Faradaic charge-transfer of MnO2. The electrochemical properties were investigated by electrochemical impedance, galvanostatic charge—discharge and cyclic voltammetry studies.

Considering its low specific surface area The cycling performance was further tested over 15 charge—discharge cycles. A dictionary consisting of commonly used terms in the green chemistry literature over the last quarter century is compiled for easy reference in a single source. The best available data sets of key parameters important for evaluating the degree of greenness of chemical processes for about first- and second-generation chemical feedstocks, including 75 solvents, relevant to life cycle, safety hazard, and energy consumption assessments are also presented.

Lavoisier numbers are introduced as a new kernel material efficiency metric analogous to process mass intensity. Geraniol, a prime constituent in the leaves of Cymbopogon martinii, has a varied range of biological activities and applications. For the selective isolation of geraniol, a newer concept of combining hydrotropic extraction with ultrasound was adopted to reduce the time of extraction and hydrotrope requirement while maintaining the quality of the product.

Sodium cumene sulfonate was selected as a suitable hydrotrope among sodium cumene sulfonate, sodium salicylate, sodium salt of para-toluene sulfonic acid, and resorcinol using the solubilization study. The screening of extraction parameters, viz. Optimization of process parameters was performed using central composite response surface design. A microscopic study was also performed to understand the extraction mechanism.


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Ultrasound assisted hydrotropic extraction turned out to be a superior sustainable alternative compared to the hydrotropic extraction because of the shortening of extraction time and reduction in hydrotrope concentration. The performance of each lithium-ion array appears strongly related to the different structural, morphological and electrochemical features of the positive electrodes. The study in full-cell of the MWCNTs anode, to date mostly investigated in lithium half-cell, is therefore performed under various conditions.

This ratio readout may be confounded by channel-specific artifacts. To maximize the utility of BLA HTS data, we analyzed the relationship between individual channels and ratio readouts after fitting 10, chemical titration series screened in seven BLA stress—response assays from the Tox21 initiative. Most Tox21 analyses adjust for this issue by evaluating target and ratio readout direction. In addition, we found that the potency and efficacy estimates derived from the ratio readouts may not represent the target channel effects and thus complicates chemical activity comparison.

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From these analyses, we recommend a simpler approach using a direct evaluation of the target and background channels as well as the respective noise levels when using BLA data for toxicity assessment. This approach eliminates the channel interference issues and allows for straightforward chemical assessment and comparisons. Transferring the mechanochemical protocol to lignin resulted in the simultaneous oxidation and cleavage of bonds with varied selectivity for monomeric products.

Finally, a scale-up approach of the oxidative procedure by using vibrating disc mill technology enabled the mechanochemical protocol to be applied in gram-scale batch reactions under reduced milling time, while affording a similar extent of oxidation. Coal-based multiscale porous carbon materials CPCs have been successfully fabricated through a friendly method with NaCl, Na2CO3, and Na2SiO3 as structural templates, instead of alkali activation at a relatively low temperature.

The optimal product CPCs obtained by the above procedure displayed a high surface area of m2 g—1. As electrode materials of supercapacitors, CPCs presented a specific capacitance of F g—1 at 1 A g—1 and superior stability over 10, cycles at 4 A g—1 owing to its hierarchical porosity with higher surface area, promoted diffusion of electrolyte, and increased conductivity. Furthermore, CPCs as the anode for Li-ion batteries exhibited a high reversible capacity of mA h g—1 at 0.


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Therefore, there are bright prospects of our CPCs as high performance electrode material for energy storage applications. A supramolecule-based ruthenium catalyst has been developed for on-water aerobic oxidation of alcohols. The catalyst showed promising efficiency with good selectivity for benzylic, propargylic, and aromatic alcohols under aqueous conditions.

propomnawaha.cf Moreover, the used catalyst was found to be easily recoverable and recyclable up to five times. Additionally, the developed oxidation methodology has been used as a key step for the total synthesis of natural product Brittonin A, including other functional group transformations such as Wittig olefination and reduction exclusively in water.

Notably, these oxidation and reduction transformations could be carried out using the developed catalyst under aqueous conditions. This unique ability of the catalyst to switch between oxidation and reduction reactions simply by changing O2 and H2 atmospheres with a balloon assembly exemplifies its versatility. To the best of our knowledge this is a first report showing the total synthesis of a molecule completely on water. This study demonstrated a simple pathway to convert underutilized biomass into valuable absorbent nanomaterials that can effectively remove cadmium II ions from water.

Conductive cellulose composites have received much attention as emerging materials due to their unique properties, such as biodegradability and flexibility. However, the achievable levels of conductivity of these cellulose composites are generally low due to the intrinsically nonconductive properties of cellulose. BaSnO3, synthesized using different amounts of dextran, has been characterized through various physicochemical techniques to understand the effect of dextran in controlling its morphology.

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The porous morphology of the rod facilitated enhanced N dye loading capability within a very short duration of 20 min. The dye adsorption behavior of the nanorod has been monitored through UV—vis absorption spectroscopy and contact angle measurements. Further, as an alternative photoanode, a DSSC of active area 0. On the basis of our results, we are able to establish porosity as an important factor in reducing the time required for effective dye adsorption which will be highly beneficial for technology development.

Critical to the functionality of energy efficient lighting, off-shore wind turbines, and electric vehicles are rare earth RE -containing phosphors and magnets. With an increase in the market penetration of these clean energy technologies, demand for RE-containing components is expected to grow. However, the production of rare earth elements REEs has an adverse impact on the environment.

Existing literature provides some information on the environmental impacts but often fails to give a detailed production pathway that can be modeled without preexisting knowledge of life cycle analysis LCA or a dedicated LCA software. Analysis of inventory data shows that electricity requirements and emissions to water have the highest contributions to the impact categories of global warming, acidification, and eutrophication.

An interconnected Excel database system is also developed to help researchers and decision makers identify environmental hotspots and develop improvements in the production pathways. Hydrogels have been used in the literature in tissue engineering, in drug delivery, and as enzyme biomimics. Herein, we report the synthesis of a functional biomaterial using BSA as scaffold and epichlorohydrin as cross-linker. The hydrogels reported in this paper were shown to exhibit tunable pore size as a function of BSA concentration by scanning electron microscopy SEM and, therefore, are well suited to encapsulate drug molecules for delivery applications.

The loading of Dox by the gel was confirmed by the emission of red fluorescence and also by filling the pores by fibrillar structures as demonstrated by SEM. Fluorescence microscopy and FACS studies support controlled and time dependent release of Dox in MCF-7 cells for 24 h where the drug goes into cytoplasm initially and then into nucleus. All of the data supports the utility of the synthesized BSA hydrogel as a biomaterial that will find application in controlled drug delivery.